4,4-bis(Dimethylamino)thiobenzophenone CAS:1226-46-6 Okuqinile okubomvu okujulile
| Inombolo Yekhathalogi | XD90453 |
| Igama Lomkhiqizo | 4,4-bis(Dimethylamino)thiobenzophenone |
| I-CAS | 1226-46-6 |
| I-Molecular Formula | I-C17H20N2OS2 |
| Isisindo samangqamuzana | 284.42 |
| Imininingwane Yesitoreji | 2 kuya ku-8 °C |
| Ikhodi Yentela Evumelanisiwe | 29309099 |
Ukucaciswa Komkhiqizo
| I-Melting Point | 202 - 206 Deg C |
| Ubumsulwa (HPLC) | 99% |
| Ekuzweleni kwegolide | Kuyavumelana |
| Ukuhlolwa kokuncibilika kwe-Chloroform | Kuyavumelana |
| Ukubukeka | Okuqinile okubomvu okujulile |
Indlela elula, inoveli futhi ebucayi ye-spectrophotometric yachazwa ukuze kunqunywe kanyekanye i-mercury ne-palladium.Indlela isekelwe ekwakhekeni okuyinkimbinkimbi kwe-mercury ne-palladium nge-Thio-Michler's Ketone (TMK) ku-pH 3.5.Zonke izici ezithinta ukuzwela zathuthukiswa futhi ububanzi obuguquguqukayo bomugqa bokunqunywa kwe-mercury ne-palladium kwatholakala.Ukunqunywa ngesikhathi esisodwa kwezingxube ze-mercury ne-palladium ngokusebenzisa indlela ye-spectrophotometric kuyinkinga enzima, ngenxa yokuphazamiseka kwe-spectral.Ngezindlela zokulinganiswa kwe-multivariate njengezikwele ezincane (i-PLS), kungenzeka ukuthola imodeli elungiselwe amanani okugxilisa izingxube ezisetshenziswa ebangeni lokulinganisa.Ukulungiswa kwesignali ye-Orthogonal (OSC) kuyindlela yokucubungula kusengaphambili esetshenziselwa ukususa ulwazi olungahlobene nokuguquguqukayo okuqondiwe okusekelwe ekuhlaziyweni kwengxenye eyinhloko ebambezelekile.I-OSC iyindlela efanelekile yokucubungula kusengaphambili yokulinganiswa kwe-PLS kwezingxube ngaphandle kokulahlekelwa umthamo wokuqagela kusetshenziswa indlela ye-spectrophotometric.Kulolu cwaningo, imodeli yokulinganisa isuselwe ku-spectra yokumuncwa ebangeni le-360-660 nm yezingxube ezihlukene ezingama-25 ze-mercury ne-palladium.Omatikuletsheni bokulinganisa bebequkethe u-0.025-1.60 kanye no-0.05-0.50 microg mL(-1) we-mercury ne-palladium, ngokulandelanayo.I-RMSEP ye-mercury ne-palladium ene-OSC futhi ngaphandle kwe-OSC yayingu-0.013, 0.006 kanye no-0.048, 0.030, ngokulandelanayo.Le nqubo ivumela ukuzimisela kanyekanye kwe-mercury ne-palladium kumasampuli okwenziwa kanye ne-matrix yangempela ukwethembeka okuhle kokuzimisela.
